HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonic acid → HCID 87222855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | 4-Methyl-3H-benzooxazol-2-one | HCID 12709336 | — |
| Product | HCID 87222855 | HCID 87222855 | — |
Reaction Steps
1.10 g (6.60 mmol) 4-methyl-3H-benzoxazol-2-one in 5.0 mL (75 mmol) chlorosulphonic acid were stirred for 2 h at RT. Then the reaction mixture was very slowly added dropwise to a large amount of ice and stirred at RT. The precipitate formed was suction filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-a9cf64af717b4eee91500c6b45411654 |
| Source note | uspto-grants-2015_02 |