HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86663906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,6-Dichloro-2-methylpyrimidine | HCID 234997 | — |
| Reactant | 6-hydroxy-4-methylbenzo[d]oxazol-2(3H)-one | HCID 66978093 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86663906 | HCID 86663906 | — |
Reaction Steps
100 mg (0.724 mmol) potassium carbonate and 110 mg (0.655 mmol) 4,6-dichloro-2-methyl-pyrimidine were added to 100 mg (0.575 mmol) 6-hydroxy-4-methyl-3H-benzoxazol-2-one in 1.5 mL DMF and the mixture was stirred for 2 h at RT. Then 15 mL water were added and the mixture was stirred overnight at RT. The precipitate formed was suction filtered, washed with water and dried i. vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-f9a7d0a08fda4b09b0e8818a014a419b |
| Source note | uspto-grants-2015_02 |