HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxyacetic Acid → 2-(methoxymethyl)-4-methyl-1H-benzo[d]imidazol-6-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxyacetic Acid | HCID 12251 | — |
| Reactant | 3,4-Diamino-5-methylphenol | HCID 19907644 | — |
| Product | 2-(methoxymethyl)-4-methyl-1H-benzo[d]imidazol-6-ol | HCID 66978239 | — |
Reaction Steps
0.55 g (4.00 mmol) 3,4-diamino-5-methyl-phenol and 1.57 mL (20.00 mmol) methoxy-acetic acid were stirred for 1 h at 120° C. Then the reaction mixture was evaporated down and further reacted as crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-0a9782ae3d6c474b9a96289133f1de66 |
| Source note | uspto-grants-2015_02 |