Diisopropylethylamine → HCID 178432265, compound

Participants

Reaction Steps

150 mg (0.548 mmol) (6-chloro-pyrimidin-4-yl)-(2,7-dimethyl-1H-benzimidazol-5-yl)-amine, 150 mg (0.559 mmol) 3-piperidin-4-yl-1,3-dihydro-imidazo[4,5-c]quinolin-2-one and 1.00 mL (5.81 mmol) DIPEA were refluxed in 1.0 mL DMF. After the reaction had ended the reaction mixture was diluted with MeOH and purified by preparative HPLC. The product-containing fractions were combined and freeze-dried.

Provenance & Evidence