Benzoyl chloride, 3-chloro- → HCID 67341197, compound

Participants

Reaction Steps

To a solution of 0.029 g (0.10 mmol) of 4-(2-piperidin-1-yl-ethyl)-3,4,5,6-tetrahydro-2H-[1,2′]bipyridinyl-3′-ylamine in N,N-dimethylformamide (1 mL) is added 0.017 g (0.10 mmol) of 3-chlorobenzoyl chloride. The mixture is stirred at room temperature for 6 hours and then purified by preparative reverse phase HPLC to provide 0.015 g (35%) of the title compound (44) as a colorless solid. [M+H]+=427.1.

Provenance & Evidence