huagongshe.com
HRID1846840

反应详情

EQUATION

反应方程式

HRID 1846840 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccccc1S(=O)(=O)Cl
HCID8623

Toluene-2-sulphonyl chloride

C7H7ClO2S

结构：NCc1cc(=O)c(OCc2ccccc2)co1
HCID21524753

未命名化合物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2)occ1OCc1ccccc1
HCID86725690

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccccc1S(=O)(=O)NCc1cc(=O)c(OCc2ccccc2)co1
HCID86725698

未命名化合物

收率 64.32%

PROCEDURE

实验过程

N-(5-Benzyloxy-4-oxo-4H-pyran-2-ylmethyl)-2-methyl-benzenesulfonamide (7-02) (22.0 g, 64.32%) was synthesized as a light brown solid from 2-aminomethyl-5-benzyloxy-pyran-4-one (5) (20.5 g, 88.74 mmol) and 2-methyl-benzenesulfonyl chloride (6-02) (20.23 g, 106.49 mmol) following the procedure described for N-(5-benzyloxy-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (7-01).