HRID1846843

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2)oc(CO)c1OCc1ccccc1

HCID86725693

未命名化合物

结构：Cc1ccccc1S(=O)(=O)NCc1cc(=O)c(O)c(CO)o1

HCID86725700

未命名化合物

PRODUCTS

生成物

结构：Cc1ccccc1S(=O)(=O)NCc1cc(=O)c(OCc2ccccc2)c(CO)o1

HCID86725701

未命名化合物

收率 40.85%

PROCEDURE

实验过程

N-(5-Benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-2-methyl-benzenesulfonamide (10-02) (4.7 g, 40.85%) was synthesized as a white solid from N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-2-methyl-benzenesulfonamide (9-02) (9.0 g, 27.69 mmol) following the procedure described for N-(5-benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (10-01).