HRID1846847

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：Cc1ccccc1S(=O)(=O)NCc1cc(=O)c(OCc2ccccc2)c(C(=O)O)n1C

HCID86725704

未命名化合物

结构：Cn1c(CNS(=O)(=O)c2ccccc2)cc(=O)c(O)c1C(=O)O

HCID86725706

未命名化合物

PRODUCTS

生成物

结构：Cc1ccccc1S(=O)(=O)NCc1cc(=O)c(O)c(C(=O)O)n1C

HCID86725705

未命名化合物

收率 9.41%

PROCEDURE

实验过程

3-Hydroxy-1-methyl-4-oxo-6-[(toluene-2-sulfonylamino)-methyl]-1,4-dihydro-pyridine-2-carboxylic acid (30.0 mg, 9.41%, purified by Prep-HPLC) was synthesized as an off white solid from 3-benzyloxy-1-methyl-4-oxo-6-[(toluene-2-sulfonylamino)-methyl]-1,4-dihydro-pyridine-2-carboxylic acid (13-02) (400.0 mg, 0.905 mmol) following the procedure described for 6-(benzenesulfonylamino-methyl)-3-hydroxy-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (14-02).