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HRID1846850

反应详情

EQUATION

反应方程式

HRID 1846850 的结构方程式

REACTANTS

反应物

2
结构：O=c1cc(CNS(=O)(=O)c2ccccc2)oc(CO)c1O
HCID86725692

未命名化合物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2Cl)occ1O
HCID86725708

未命名化合物

PRODUCTS

生成物

1
结构：O=c1cc(CNS(=O)(=O)c2ccccc2Cl)oc(CO)c1O
HCID86725709

未命名化合物

收率 48.59%

PROCEDURE

实验过程

2-Chloro-N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (9-03) (8.0 g, 48.59%) was synthesized as a white solid from 2-chloro-N-(5-hydroxy-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (8-03) (15.0 g, 47.61 mmol) following the procedure described for N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (9-01).