HRID1846851

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2)oc(CO)c1OCc1ccccc1

HCID86725693

未命名化合物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2Cl)oc(CO)c1O

HCID86725709

未命名化合物

PRODUCTS

生成物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2Cl)oc(CO)c1OCc1ccccc1

HCID86725710

未命名化合物

收率 35%

PROCEDURE

实验过程

N-(5-Benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-2-chloro-benzenesulfonamide (10-03) (3.5 g, 35.0%) was synthesized as a white solid from 2-chloro-N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (9-03) (8.0 g, 23.18 mmol) following the procedure described for N-(5-benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (10-01).