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HRID1846855

反应详情

EQUATION

反应方程式

HRID 1846855 的结构方程式

REACTANTS

反应物

2
结构：Cn1c(C(N)S(=O)(=O)c2ccccc2)cc(=O)c(O)c1C(=O)O
HCID86725697

未命名化合物

结构：Cn1c(CNS(=O)(=O)c2ccccc2Cl)cc(=O)c(OCc2ccccc2)c1C(=O)O
HCID86725713

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c(CNS(=O)(=O)c2ccccc2Cl)cc(=O)c(O)c1C(=O)O
HCID76073528

未命名化合物

收率 37.2%

PROCEDURE

实验过程

6-[(2-Chloro-benzenesulfonylamino)-methyl]-3-hydroxy-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (14-03) (120.0 mg, 37.18%, purified by Prep-HPLC) was synthesized as a white solid from 3-benzyloxy-6-[(2-chloro-benzenesulfonylamino)-methyl]-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (13-03) (400.0 mg, 0.866 mmol) following the procedure described for 6-(benzenesulfonylamino-methyl)-3-hydroxy-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (14-01).