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HRID1846863

反应详情

EQUATION

反应方程式

HRID 1846863 的结构方程式

REACTANTS

反应物

2
结构：Cn1c(C(N)S(=O)(=O)c2ccccc2)cc(=O)c(O)c1C(=O)O
HCID86725697

未命名化合物

结构：Cc1cccc(S(=O)(=O)NCc2cc(=O)c(OCc3ccccc3)c(C(=O)O)n2C)c1
HCID86725720

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cccc(S(=O)(=O)NCc2cc(=O)c(O)c(C(=O)O)n2C)c1
HCID86725721

未命名化合物

收率 29%

PROCEDURE

实验过程

3-Hydroxy-1-methyl-4-oxo-6-[(toluene-3-sulfonylamino)-methyl]-1,4-dihydro-pyridine-2-carboxylic acid (14-04) (60.0 mg, 28.41%, purified by Prep-HPLC) was synthesized as an off white solid from 3-benzyloxy-1-methyl-4-oxo-6-[(toluene-3-sulfonylamino)-methyl]-1,4-dihydro-pyridine-2-carboxylic acid (13-04) (260.0 mg, 0.588 mmol) following the procedure described for 6-(benzenesulfonylamino-methyl)-3-hydroxy-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (14-01).