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HRID1846866

反应详情

EQUATION

反应方程式

HRID 1846866 的结构方程式

REACTANTS

反应物

2
结构：O=c1cc(CNS(=O)(=O)c2ccccc2)oc(CO)c1O
HCID86725692

未命名化合物

结构：O=c1cc(CNS(=O)(=O)c2cccc(Cl)c2)occ1O
HCID86725723

未命名化合物

PRODUCTS

生成物

1
结构：O=c1cc(CNS(=O)(=O)c2cccc(Cl)c2)oc(CO)c1O
HCID86725724

未命名化合物

收率 47.5%

PROCEDURE

实验过程

3-Chloro-N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (9-05) (7.3 g, 47.50%) was synthesized as a white solid from 3-chloro-N-(5-hydroxy-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (8-05) (14.0 g, 44.44 mmol) following the procedure described for N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (9-01).