HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(5-hydroxy-4-oxo-4H-pyran-2-ylmethyl)-benzene sulfonamide → N-(5-Hydroxy-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(5-hydroxy-4-oxo-4H-pyran-2-ylmethyl)-benzene sulfonamide | HCID 86725691 | — |
| Reactant | N-(5-Benzyloxy-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide | HCID 86725730 | — |
| Product | N-(5-Hydroxy-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide | HCID 86725731 | 73% |
Reaction Steps
N-(5-Hydroxy-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide (8-06) (14.0 g, crude) was synthesized as a light brown solid from N-(5-benzyloxy-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide (7-06) (25.0 g, 64.93 mmol) following the procedure described for N-(5-hydroxy-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (8-01).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952039B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-35f6b7086e98452389ae2f3fe915d4d9 |
| Source note | uspto-grants-2015_02 |