HRID1846875

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2)oc(CO)c1OCc1ccccc1

HCID86725693

未命名化合物

结构：Cc1ccc(S(=O)(=O)NCc2cc(=O)c(O)c(CO)o2)cc1

HCID86725732

未命名化合物

PRODUCTS

生成物

结构：Cc1cccc(S(=O)(=O)NCc2cc(=O)c(OCc3ccccc3)c(CO)o2)c1

HCID86725717

未命名化合物

收率 41.35%

PROCEDURE

实验过程

N-(5-Benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-3-methyl-benzenesulfonamide (10-06) (3.7 g, 41.35%) was synthesized as a white solid from N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide (9-06) (7.0 g, 21.54 mmol) following the procedure described for N-(5-benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (10-01).