HRID1846876

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=Cc1oc(CNS(=O)(=O)c2ccccc2)cc(=O)c1OCc1ccccc1

HCID86725694

未命名化合物

结构：Cc1cccc(S(=O)(=O)NCc2cc(=O)c(OCc3ccccc3)c(CO)o2)c1

HCID86725717

未命名化合物

PRODUCTS

生成物

结构：Cc1ccc(S(=O)(=O)NCc2cc(=O)c(OCc3ccccc3)c(C=O)o2)cc1

HCID86725733

未命名化合物

收率 59.62%

PROCEDURE

实验过程

N-(5-Benzyloxy-6-formyl-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide (11-06) (2.2 g, 59.62%) was synthesized as a yellow sticky solid from N-(5-benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-4-methyl-benzenesulfonamide (10-06) (3.7 g, 8.92 mmol) following the procedure described for N-(5-benzyloxy-6-formyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (11-01).