HRID1846883

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=c1cc(CNS(=O)(=O)c2ccccc2)oc(CO)c1OCc1ccccc1

HCID86725693

未命名化合物

结构：O=c1cc(CNS(=O)(=O)c2ccc(Cl)cc2)oc(CO)c1O

HCID86725739

未命名化合物

PRODUCTS

生成物

结构：O=c1cc(CNS(=O)(=O)c2ccc(Cl)cc2)oc(CO)c1OCc1ccccc1

HCID86725740

未命名化合物

收率 46.17%

PROCEDURE

实验过程

N-(5-Benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-4-chloro-benzenesulfonamide (10-07) (3.5 g, 46.17%) was synthesized as a white solid from 4-chloro-N-(5-hydroxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (9-07) (6.0 g, 17.39 mmol) following the procedure described for N-(5-benzyloxy-6-hydroxymethyl-4-oxo-4H-pyran-2-ylmethyl)-benzenesulfonamide (10-01).