HRID1846887

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：Cn1c(C(N)S(=O)(=O)c2ccccc2)cc(=O)c(O)c1C(=O)O

HCID86725697

未命名化合物

结构：Cn1c(CNS(=O)(=O)c2ccc(Cl)cc2)cc(=O)c(OCc2ccccc2)c1C(=O)O

HCID86725743

未命名化合物

PRODUCTS

生成物

结构：Cn1c(CNS(=O)(=O)c2ccc(Cl)cc2)cc(=O)c(O)c1C(=O)O

HCID86725744

未命名化合物

收率 31.6%

PROCEDURE

实验过程

6-[(4-Chloro-benzenesulfonylamino)-methyl]-3-hydroxy-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (14-07) (140.0 mg, 31.55%) was synthesized as a brown solid from 3-benzyloxy-6-[(4-chloro-benzenesulfonylamino)-methyl]-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (13-07) (550.0 mg, 1.19 mmol) following the procedure described for 6-(benzenesulfonylamino-methyl)-3-hydroxy-1-methyl-4-oxo-1,4-dihydro-pyridine-2-carboxylic acid (14-01).