HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1,1'-(benzene-1,3-diyldimethanediyl)bis(1H-pyrrole-2,5-dione)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | 1,3-Benzenedimethanamine | HCID 15133 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Product | 1,1'-(benzene-1,3-diyldimethanediyl)bis(1H-pyrrole-2,5-dione) | HCID 22712661 | — |
Reaction Steps
The general procedure was carried out using maleic anhydride (20.59 g, 210 mmol), m-xylylenediamine (13.62 g, 100 mmol), sodium acetate (1.64 g, 20 mmol), and acetic anhydride (22.46 g, 220 mmol). The resulting compound was purified by column chromatography (97:3 DCM:EtOAc), and the product obtained as a white solid (6.51 g/22%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952094B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-caf7cca73ca44c8bba8a9b2850773d9d |
| Source note | uspto-grants-2015_02 |