HCID 67609415, compound → HCID 68008633, compound

Participants

Reaction Steps

Compound 95 (16.7 mg, 0.0425 mmol) obtained in Example 67 was dissolved in allylbromide (2 mL), and silver oxide (986 mg, 4.25 mmol) was added thereto, followed by stirring under light shading at room temperature for 14 hours. Silver oxide was separated by filtration, the filtrate was concentrated, and the residue was purified by silica gel column chromatography (33% ethyl acetate/n-hexane) to obtain the title compound (3.7 mg, 21%).

Provenance & Evidence