HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethoxy)benzylamine → HCID 86728207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethoxy)benzylamine | HCID 145264 | — |
| Reactant | 3-Fluoropyridine-4-carboxylic acid | HCID 345361 | — |
| Product | HCID 86728207 | HCID 86728207 | 4% |
Reaction Steps
The title compound was prepared in 4% yield from 3-trifluoromethoxy-benzylamine and 3-fluoroisonicotinic acid according to the procedure for the preparation of Example 3. 1H NMR (400 MHz, DMSO-d6): δ 13.47 (br s, 1H), 8.11 (br s, 1H), 7.84 (br s, 1H), 7.59 (s, 1H), 7.24-7.51 (m, 4H), 4.64 (s, 2H). [M+H] calc'd for C14H11F3N2O3, 313. Found 313.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952151B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-ad3e74a441674f9fa7620738b7bc9c61 |
| Source note | uspto-grants-2015_02 |