Tetramethyltin → HCID 136343993, compound

HRID 1847288Notes

Reaction equation

HRID 1847288 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[C:7]([OH:22])=[C:8]2[C:15]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[N:14][S:13][C:9]2=[C:10](Br)[N:11]=1)=[O:5])[CH3:2].[CH3:23][Sn](C)(C)C>>[CH2:1]([O:3][C:4]([C:6]1[C:7]([OH:22])=[C:8]2[C:15]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[N:14][S:13][C:9]2=[C:10]([CH3:23])[N:11]=1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 11661TetramethyltinHCID 136344015HCID 136344015, compound

Product 1

HCID 136343993HCID 136343993, compound

Procedure

Prepared in analogy to Example 36 from 7-bromo-4-hydroxy-3-phenyl-isothiazolo[5,4-c]pyridine-5-carboxylic acid ethyl ester and tetramethyltin; MS (m/z): 315.32 (M+H+).

Sources & evidence

ORD record
ord-10af87cf26354a63b2bf52c3412b74af
Source dataset
uspto-grants-2015_02
Patent number
US08952160B2

Reaction notes

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