HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl isocyanate → HCID 66778751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 56847101 | HCID 56847101 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 66778751 | HCID 66778751 | — |
Reaction Steps
To a vial containing benzyl isocyanate (0.0166 g, 0.125 mmol), was added methyl 5,6,7,8-tetrahydro-1,6-naphthyridine-2-carboxylate hydrochloride (0.0220 g, 0.0962 mmol), DIPEA (0.0586 mL, 0.337 mmol) and DMF (2 mL). The resulting solution was then shaken at rt for 13 h and then concentrated to give methyl 6-(benzylcarbamoyl)-5,6,7,8-tetrahydro-1,6-naphthyridine-2-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952163B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-93374b812bee43179258991537c1f28d |
| Source note | uspto-grants-2015_02 |