HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1R,3R)-3-Aminocyclohexane-1-carboxylic acid 2,2,2-trifluoroacetic acid salt → ((1R,3R)-3-Aminocyclohexyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1R,3R)-3-Aminocyclohexane-1-carboxylic acid 2,2,2-trifluoroacetic acid salt | HCID 86681198 | — |
| Reactant | HCID 178479263 | HCID 178479263 | — |
| Product | ((1R,3R)-3-Aminocyclohexyl)methanol | HCID 55284699 | — |
Reaction Steps
((1R,3R)-3-Aminocyclohexyl)methanol was synthesized as a white powder (213 mg, 75%) using a procedure analogous to that described in Step 1 of Example 179, substituting (1R,3R)-3-aminocyclohexanecarboxylic acid trifluoroacetate from the previous step for trans-4-aminocyclohexanecarboxylic acid hydrochloride used in Example 179.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952058B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-9071586c0a234dc1aca2ff05541e819d |
| Source note | uspto-grants-2015_02 |