Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1403835-45-9 | HCID 70941112 | — |
| Solvent | Water | HCID 962 | — |
| Product | S 38093-2 | HCID 70945946 | 89% |
Reaction Steps
14.69 kg of 4-{3-[cis-hexahydrocyclopenta[c]pyrrol-2(1H)-yl]propoxy}benzamide and 122 L of water are introduced into a reactor. A solution of 6.81 kg of 37% hydrochloric acid in 11.54 L of water is also prepared. 13.75 kg of this acid solution are added to the reactor. The mixture is stirred for 1 hour at ambient temperature, and then for 1 hour 30 minutes at 60° C. The suspension is filtered in the hot state and the filter is then rinsed with water. A solvent change is then carried out on the filtrate, keeping the volume constant, in order to obtain an isopropanol/water ratio of 9/1. The product is isolated at 0° C. and the precipitate obtained is washed with isopropanol. The title product is finally obtained in a yield of 89% and with a chemical purity greater than 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08952179B2 |
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| Source dataset | uspto-grants-2015_02 |
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| ORD ID | ord-8ef778aaf3024affa7d04abbc9559fcc |
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| Source note | uspto-grants-2015_02 |
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