HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 86675647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | Acrylate | HCID 25188 | — |
| Reactant | 2-Ethyl-2-(hydroxymethyl)propane-1,3-diol;prop-2-enoic acid | HCID 25019176 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86675647 | HCID 86675647 | — |
Reaction Steps
N-methylaniline (14.81 g) was added to glacial acetic acid (25 ml) containing trimethylolpropane triacrylate (16.05 g) and the mixture heated under reflux for 12 hr. The acetic acid was removed by distillation in vacuo to give a viscous oil. An infrared spectrum of the product showed that very few acrylate residues were present. Strong absorptions due to an ester and an aromatic amine group were present (1740 and 1600 cm−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952190B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-812b6d45ec4e4c57a6a118a963507476 |
| Source note | uspto-grants-2015_02 |