HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 1-(Oxan-4-yl)piperidin-4-amine dihydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | tert-butyl N-[1-(oxan-4-yl)piperidin-4-yl]carbamate | HCID 45792109 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 1-(Oxan-4-yl)piperidin-4-amine dihydrochloride | HCID 45156751 | — |
Reaktionsschritte
A solution of EXAMPLE 49A (52.57 g) in dichloromethane (900 mL) was treated with 4M aqueous HCl (462 mL), mixed vigorously at room temperature for 16 hours and concentrated.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08952157B2 |
| Quelldatensatz | uspto-grants-2015_02 |
| ORD ID | ord-2fd778e07d3a4ec5b34cb3cc13935c2e |
| Quellennotiz | uspto-grants-2015_02 |