HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 4-((2-cyanoadamantan-2-yl)methoxy)-5-cyclopropyl-2-fluorobenzoate → HCID 86703731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 4-((2-cyanoadamantan-2-yl)methoxy)-5-cyclopropyl-2-fluorobenzoate | HCID 86703654 | — |
| Reactant | HCID 86703732 | HCID 86703732 | — |
| Product | HCID 86703731 | HCID 86703731 | — |
Reaction Steps
Following the procedure as described in Example 332 Step 6, and making variations as required to replace tert-butyl 4-((2-cyanoadamantan-2-yl)methoxy)-5-cyclopropyl-2-fluorobenzoate with tert-butyl 5-cyclopropyl-4-((1-(difluoromethyl)-cyclohexyl)methoxy)-2-fluorobenzoate, the title compound was obtained as a beige solid (0.16 g, 96%): MS (ES+) m/z 343.1 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952169B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-a26f5777f10e48b391ae740a36c10831 |
| Source note | uspto-grants-2015_02 |