Hydrochloric Acid → Hydrochloric Acid

Participants

Reaction Steps

(S)-tert-butyl 1-(3-(cyclopentyloxy)phenyl)ethylcarbamate (75.1 mg, 0.246 mmol) was dissolved in 4M HCl in dioxane (1 ml, 4.00 mmol) and the resulting mixture was allowed to sit for 1 hour, then concentrated to yield (S)-1-(3-(cyclopentyloxy)phenyl)ethanamine as an HCl salt (yield assumed quantitative). LCMS m/z 206.1 (M+H)+, Rt 0.61 min.

Provenance & Evidence