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HRID1851175

反应详情

EQUATION

反应方程式

HRID 1851175 的结构方程式

REACTANTS

反应物

2
结构：O=C1CCC(=O)N1Br
HCID67184

1-Bromopyrrolidine-2,5-dione

C4H4BrNO2

结构：O=Cc1ccc(-c2nc3nccn3cc2-c2ccccc2)cc1
HCID86630655

未命名化合物

PRODUCTS

生成物

1
结构：O=Cc1ccc(-c2nc3ncc(Br)n3cc2-c2ccccc2)cc1
HCID86630658

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

1.5 g 4-(6-phenylimidazo[1,2-a]pyrimidin-7-yl)benzaldehyde and 0.9 g NBS were refluxed in 30 mL chloroform for 1 h. The solvent was removed by distillation and the crude product was purified by column chromatography (dichloromethane/methanol).

WORKUP

后处理

  1. customThe solvent was removed by distillation
  2. customthe crude product was purified by column chromatography (dichloromethane/methanol)