HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(5-Azetidine-3-yl-[1,2,4]triazole-3-yl)-6-methylpyridine → HCID 178498702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(5-Azetidine-3-yl-[1,2,4]triazole-3-yl)-6-methylpyridine | HCID 68753485 | — |
| Reactant | HCID 86703062 | HCID 86703062 | — |
| Product | HCID 178498702 | HCID 178498702 | 9.7% |
Reaction Steps
The title compound has been prepared in analogy to the aforementioned descriptions by reacting 500 mg (1.4 mmol) 7-(4-formylphenyl)-6-phenyl-imidazo[1,2-a]pyrimidine-2-carboxylic acid methyl ester with 671.9 mg (1.4 mmol) 2-(5-azetidine-3-yl-[1,2,4]triazole-3-yl)-6-methylpyridine×2HCl (60% pure), yielding 75.6 mg (9.2%) of the desired product after purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957064B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-3b6f823e6f3f4b0089714e0db53a290f |
| Source note | uspto-grants-2015_02 |