Hydrogen Bromide → HCID 86702638, compound

Participants

Reaction Conditions

Reaction Steps

4 (0.802 g, 2.94 mmol) was placed into a round bottom flask. Hydrobromic acid (18 mL of a 48 wt % aqueous solution) was added. Concentrated sulfuric acid (3 mL) was added dropwise to the stirring mixture. The reaction mixture was heated to 80° C. for 3 hours. The reaction mixture was allowed to cool and contents filtered. The resulting solids were dried for 30 minutes and the solid was slurried in diethyl ether. Most of the solids dissolved to give a yellow solution. The solution was dried over MgSO4 and filtered. The volatiles were removed under vacuum to give a yellow sticky solid (1.01 g, 100% yield).

Provenance & Evidence