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HRID1851732

反应详情

EQUATION

反应方程式

HRID 1851732 的结构方程式

REACTANTS

反应物

1
结构：COc1ccc(CN2CC(C=C(F)F)C(C(=O)O)C2=O)c(OC)c1
HCID58019132

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(CN2CC(C=C(F)F)CC2=O)c(OC)c1
HCID58019140

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)CC(C)C
溶剂HCID7909

4-Methyl-2-pentanone

C6H12O

CONDITIONS

反应条件

温度
116 °C

PROCEDURE

实验过程

A suspension of (K) in methyl isobutyl ketone (MIBK-5 L) is heated at 116° C. overnight. Evaporation of the solvent gives 564 g of (IIIc). The product is used in the next reaction without further purification.

WORKUP

后处理

  1. customEvaporation of the solvent
  2. customgives 564 g of (IIIc)
  3. customThe product is used in the next reaction without further purification