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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1851861Generated: October 25, 2026

L-Valinol → N-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinol

https://huagongshe.com/reaction/1851861

Reaction equation

Participants

RoleNameHCIDCharge
ReactantL-ValinolHCID 640993—
Reactant1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acidHCID 57672890—
ProductN-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinolHCID 24875907—

Reaction Steps

2.00 g (7.48 mmol) of 1-[[(2-furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acid was used instead of 2-benzothiophenecarboxylic acid and 772 mg (7.48 mmol) of L-valinol was used instead of 1-aminocyclohexanecarboxylic acid phenylmethyl ester in the process according to Reference example 188 to obtain 2.64 g (quantitative) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08957205B2
Source datasetuspto-grants-2015_02
ORD IDord-4c940c716eba426fb5e27dede4b5b95d
Source noteuspto-grants-2015_02