HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Valinol → N-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Valinol | HCID 640993 | — |
| Reactant | 1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acid | HCID 57672890 | — |
| Product | N-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinol | HCID 24875907 | — |
Reaction Steps
2.00 g (7.48 mmol) of 1-[[(2-furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acid was used instead of 2-benzothiophenecarboxylic acid and 772 mg (7.48 mmol) of L-valinol was used instead of 1-aminocyclohexanecarboxylic acid phenylmethyl ester in the process according to Reference example 188 to obtain 2.64 g (quantitative) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08957205B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-4c940c716eba426fb5e27dede4b5b95d |
| Source note | uspto-grants-2015_02 |