反应详情

温度

100 °C

A mixture of 24.5 g morpholine and 13.3 g 1-Fluoro-4-nitro-benzene in 30 mL DMSO was heated to 100° C. for 4 h. This solution was poured on to 300 mL of water and the resulting precipitate was collected by filtration to yield a bright yellow crystalline product, which was dried under reduced pressure. Yield: 19.7 g.

1. filtrationthe resulting precipitate was collected by filtration
2. customto yield a bright yellow crystalline product, which
3. customwas dried under reduced pressure