HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Benzodioxan-6-ylamine → HCID 86689321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Benzodioxan-6-ylamine | HCID 89148 | — |
| Reactant | HCID 86689304 | HCID 86689304 | — |
| Product | HCID 86689321 | HCID 86689321 | 98.1% |
Reaction Steps
1-Nitro-5,6,7,8-tetrahydronaphthalen-2-yl triflate (3.25 g, 10 mmol) and 6-amino-2,3-dihydrobenzo[1,4]dioxin (1.51 g, 10 mmol) were used in a process similar to Example 1(1) to give the titled compound as red oil (3.20 g, yield 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962613B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-49b9c37b0a6d42f2807198f5ba04551a |
| Source note | uspto-grants-2015_02 |