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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1852585Generated: October 30, 2026

Potassium Carbonate → HCID 59633880, compound

https://huagongshe.com/reaction/1852585

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 59633877HCID 59633877—
SolventMethanolHCID 887—
SolventWaterHCID 962—
ProductHCID 59633880HCID 59633880102%

Reaction Conditions

Temperature75 °C

Reaction Steps

A solution of 95 mg (0.32 mmol) of compound 9m was combined with 120 mg (0.87 mmol) of K2CO3 in 8 mL of MeOH and heated at 75° C. for 5 h. The mixture was cooled, diluted with water, and extracted with CH2Cl2. The organic solution was concentrated to give 100 mg (100%) of 9n as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962607B2
Source datasetuspto-grants-2015_02
ORD IDord-db22ec1412404d8da633b9aa9d3a11d5
Source noteuspto-grants-2015_02