HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-3-methoxybenzene → HCID 136352225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-3-methoxybenzene | HCID 640753 | — |
| Reactant | HCID 86673023 | HCID 86673023 | — |
| Product | HCID 136352225 | HCID 136352225 | — |
Reaction Steps
2-isoquinolin-3-yl-7-(3-methoxyphenyl)ethynyl-chromen-4-one oxime was prepared in 22% overall yield using the method described in example 24, starting from 7-bromo-2-isoquinolin-3-yl-chromen-4-one O-tert-butyl oxime (example 2B) and 3-methoxyphenylacetylene. The title compound was isolated as an orange solid and as a 93/7 mixture of Z/E oxime isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962627B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-8864432b1ce14724a3a75e75d87793fb |
| Source note | uspto-grants-2015_02 |