HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Ethynylphenol → HCID 136352227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Ethynylphenol | HCID 139144 | — |
| Reactant | HCID 86673023 | HCID 86673023 | — |
| Product | HCID 136352227 | HCID 136352227 | — |
Reaction Steps
7-(3-hydroxyphenyl)ethynyl-2-isoquinolin-3-yl-chromen-4-one oxime was prepared in 28% overall yield using the method described in example 24, starting from 7-bromo-2-isoquinolin-3-yl-chromen-4-one O-tert-butyl oxime (example 2B) and 3-hydroxyphenylacetylene. The title compound was isolated as a yellow solid and as a 80/20 mixture of Z/E oxime isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962627B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-dc88636ad6aa42e6a7672aafe0207067 |
| Source note | uspto-grants-2015_02 |