HCID 2392279, compound → HCID 49872630, compound

Participants

Reaction Steps

3-Amino-6-ethylthieno[2,3-d]pyrimidin-4(3H)-one and 1-adamantane acetyl chloride were reacted as described in Example 5 to provide the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm. 35 (t, J=7.5 Hz, 1H), 1.64-1.73 (m, 12H), 2.00-2.04 (m, 3H), 2.21 (s, 2H), 2.88 (qd, J=7.5, 1.2 Hz, 1H), 7.17 (t, J=1.2 Hz, 1H), 7.93 (s, 1H), 8.08 (s, 1H) ppm; MS (DCI/NH3) m/z 372 (M+H)+; Elemental Analysis: Calculated for C20H25N3O2S.0.2H2O: C, 64.04; H, 6.83; N, 11.20. Found: C, 63.91; H, 6.68; N, 11.27.

Provenance & Evidence