HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 9-Bromo-8-methoxy-2-methylthieno[2,3-c]quinolin-4(5H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 8-Methoxy-2-methylthieno[2,3-c]quinolin-4(5H)-one | HCID 67447573 | — |
| Product | 9-Bromo-8-methoxy-2-methylthieno[2,3-c]quinolin-4(5H)-one | HCID 67450116 | 40% |
Reaction Steps
Following Step 4 from General Procedure A, 8-methoxy-2-methylthieno[2,3-c]quinolin-4(5H)-one (1.4 g, 5.7 mmol) was reacted with N-bromosuccinimide (1.2 g, 6.9 mmol) to afford the desired product (740 mg, 40%) as a brown solid: ESI MS m/z 325 [C13H10BrNO2S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-0d74003604b54b3aaa9853ee896dd0be |
| Source note | uspto-grants-2015_02 |