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HRID1853665

反应详情

EQUATION

反应方程式

HRID 1853665 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1Br
HCID67449139

未命名化合物

结构：C[C@H](CN(C)C(=O)OC(C)(C)C)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1
HCID67452101

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1-c1ccc([C@H](C)CN(C)C(=O)OC(C)(C)C)cc1
HCID67447279

未命名化合物

收率 50%

PROCEDURE

实验过程

Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (2.5 g, 8.1 mmol) was reacted with (S)-tert-butylmethyl(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)propyl)carbamate (4.6 g, 12 mmol) to afford the desired product (1.9 g, 50%) as a light brown solid: ESI MS m/z 47 [C27H30N2O4S+H]+.