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HRID1853668

反应详情

EQUATION

反应方程式

HRID 1853668 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1Br
HCID67449139

未命名化合物

结构：CC(C)(C)OC(=O)NCCc1ccc(B2OC(C)(C)C(C)(C)O2)cc1Cl
HCID67452738

Carbamic acid, N-[2-[2-chloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]ethyl]-, 1,1-dimethylethyl ester

C19H29BClNO4

PRODUCTS

生成物

1
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1-c1ccc(CCNC(=O)OC(C)(C)C)c(Cl)c1
HCID89682133

未命名化合物

收率 57%

PROCEDURE

实验过程

Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (3.0 g, 9.7 mmol) was reacted with tert-butyl 2-chloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate (5.53 g, 14.5 mmol) to afford the desired product (2.65 g, 57%) as a light brown solid. ESI MS m/z 485 [C25H25ClN2O4S+H]+.