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HRID1853674

反应详情

EQUATION

反应方程式

HRID 1853674 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(C)c2[nH]c(=O)c3sccc3c2c1Br
HCID67450006

未命名化合物

结构：CC(C)(C)OC(=O)NCC1(c2ccc(B3OC(C)(C)C(C)(C)O3)cc2)CCC1
HCID86689569

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(C)c2[nH]c(=O)c3sccc3c2c1-c1ccc(C2(CNC(=O)OC(C)(C)C)CCC2)cc1
HCID86689520

未命名化合物

收率 45%

PROCEDURE

实验过程

Following General Procedure B, 9-bromo-8-methoxy-6-methylthieno[2,3-c]quinolin-4(5H)-one (150 mg, 0.46 mmol) was reacted with tert-butyl (1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)cyclobutyl)methylcarbamate (270 mg, 0.70 mmol to afford the desired product (105 mg, 45%) as a light brown solid: ESI MS m/z 505 [C29H32N2O4S+H]+.