HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one → HCID 86689446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one | HCID 67449139 | — |
| Reactant | HCID 86689447 | HCID 86689447 | — |
| Product | HCID 86689446 | HCID 86689446 | 40% |
Reaction Steps
Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (770 mg, 2.5 mmol) was reacted with tert-butyl ethyl(1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethyl)carbamate (1.4 g, 3.7 mmol) to afford the desired product (450 mg, 40%) as a light brown solid: ESI MS m/z 479 [C27H30N2O4S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-b4cd7a2945fc401a93bea36c4b6b5a00 |
| Source note | uspto-grants-2015_02 |