HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one → HCID 67447379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one | HCID 67449139 | — |
| Reactant | HCID 67452172 | HCID 67452172 | — |
| Product | HCID 67447379 | HCID 67447379 | 62% |
Reaction Steps
Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (500 mg, 1.6 mmol) was reacted with 2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)propanenitrile (600 g, 2.2 mmol) to afford the desired product (350 mg, 62%) as a brown solid: ESI MS m/z 361 [C21H16N2O2S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-5f68e07ab5f149e6a6e522e5eaeec4d3 |
| Source note | uspto-grants-2015_02 |