HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 67448906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 67449771 | HCID 67449771 | — |
| Product | HCID 67448906 | HCID 67448906 | 38% |
Reaction Steps
Following General Procedure 1H, tert-butyl 4-(8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)phenethylcarbamate (200 mg, 0.43 mmol) was reacted with NCS (68 mg, 0.52 mmol) to afford the desired product (79 mg, 38%) as a brown solid. ESI MS m/z 485 [C25H25ClN2O4S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-4c4c6479ec1b47a08627d03501927c64 |
| Source note | uspto-grants-2015_02 |