HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 67450206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | HCID 67448652 | HCID 67448652 | — |
| Product | HCID 67450206 | HCID 67450206 | 56.5% |
Reaction Steps
Following General Procedure H, tert-butyl 2-(4-(8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)phenyl)propylcarbamate (180 mg, 0.39 mmol) was reacted with NCS (57 mg, 0.42 mmol) to afford the desired product (110 mg, 56%) as a yellowish solid. ESI MS m/z 499 [C26H27ClN2O4S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-c28602e914dd4ea597a3b9e37b2a1a30 |
| Source note | uspto-grants-2015_02 |