HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(tert-Butylaminosulphonyl)benzeneboronic acid → HCID 67448894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(tert-Butylaminosulphonyl)benzeneboronic acid | HCID 22107170 | — |
| Reactant | 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one | HCID 67449139 | — |
| Product | HCID 67448894 | HCID 67448894 | 60.7% |
Reaction Steps
Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (5.0 g, 16 mmol) was reacted with 4-(N-tert-butylsulfamoyl)phenylboronic acid (5.4 g, 21 mmol) to afford the desired product (4.3 g, 60%) as a yellow solid: ESI MS m/z [C22H22N2O4S2+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-3968a90e920d4cea83b4fade1d4bc6f7 |
| Source note | uspto-grants-2015_02 |