HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-tert-Butoxycarbonylpiperazinyl)phenylboronic acid, pinacol ester → HCID 86689486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-tert-Butoxycarbonylpiperazinyl)phenylboronic acid, pinacol ester | HCID 2795514 | — |
| Reactant | 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one | HCID 67449139 | — |
| Product | HCID 86689486 | HCID 86689486 | 53.2% |
Reaction Steps
Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (80 mg, 0.26 mmol) was reacted with tert-butyl 4-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]piperazine-1-carboxylate (170 mg, 0.44 mmol) to afford the desired product (68 mg, 32%) as a yellow solid: ESI MS m/z 492 [C27H29N3O4S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-de2a782b89654b85aeed932141feede7 |
| Source note | uspto-grants-2015_02 |